The effect of composition of NiFe2O4 on the crystal structure of nanocomposite NiFe2O4 / PVDF that synthesized using sol gel spin coating method

Yessy Putri - Department of Physics, Universitas Negeri Padang, West Sumatera, Indonesia
- Ramli - Department of Physics, Universitas Negeri Padang, West Sumatera, Indonesia

Abstract


 

NiFe2O4 is a Ferrite Compound with the molecular formula MFe where M is a transition metal or alkaline earth is a magnetic semiconductor material with a spinel structure. The polymer used in this study is Polyvinilidene Flouride (PVDF). PVDF film is a material that is inexpensive, lightweight, flexible, has a wide frequency range, and is very sensitive. In this study 5 compositions were carried out namely ((50% : 50%), (33,3% : 66,6%), (25% : 75%), (75% : 25%), (66,6% : 33,3%)). Nanocomposites are synthesized using the sol-gel spin coating method. With making precursors (Fe(NO3) 3.9H2O and Ni(NO3) 2.6H2O. For the growth of thin films, the solution is dripped on a 0.5 cm x 0.5 cm glass substrate. Characterized using XRD (X-Rey Diffraction), SEM (Scanning Electron Microscope), FTIR (Fourier Transform Infra Red).

 

Keywords : NiFe2O4,PVDF,Nanokompocite, Sol Gel, and Spin Coating


Full Text:

PDF

References


Suryantari, Risti, dan Elok Fidiani. 2013. Materi Fisika Material. Universitas Katolik Parahiyangan : Bandung.

Chung F, Liang, J, Tao Z, dan Chen. 2010. Fungcional Materials for rechargeable.

Karokaro A, Suharpiyu, M Febri, Mujamillah ,E.Yulianti, S. Purwanto, Ridwan, Sudirman. 2002 . Aplikasi Resin Poliester Dan Epoksi Dalam Pengembangan Rigid Bonded Agnet. Jurnal Sains Materi Indonesia Vol.3 No.2. Tangerang : Puslitbang Iptek Bahan (P3IB) BATAN.

Santoso, D. R,. 2005. Design of Piezoelectric Sensor for Stress Measurement of Structural Members, Jurnal, Transaction of Japan Society of Naval Architects No. 109, Edisi Maret 2005.

Paveena, A.Z. Tachan, M. Boutbara. 2010. The Effect of Substrate Temperature on Structural and Physical Properties of Ultrasonically Sprayed Cds Film. Materials Chemistry and Physics, 94.

M. M. Hasan, A. S. M. A. Haseeb, R. Saidur, and H. H. Masjuki. 2008. Proceeding of world academy of science, Engineering and Technology. Effect of Annealing Treatment on Optical Properties of Anatase TiO2 Thin Film. Vol. 30, 1307-6884 (2008).

Riaz, R. Ashraf, A Akbar. 2014. Free Groeth Of Irone Oxide Nanostruktures by Sol-Gel Spin Coating Technique Struktural and Magnetic Properties. University Of The Punjab : Pakistan.

Naat, Jhonson Nune. 2014. Pengaruh Kecepatan Putar Deposisi Terhadap Struktur Kristal, Ketebaln, Dan Morfologi Lapisan Tipis Timbal Zirkonat Titanat (PZt) Dengan Metode Spin Coater. Chimica et Natura Acta vol 2. No 2, Austus 2014 : 115-119.

Rahmi, R., Ramli, R., & Darvina, Y. 2018 . Analisis Sifat Listrik Nanokomposit Fe3O4/PVDF Yang disentesis Dengan Metode Sol Gel Untuk Aplikasi Elektroda Baterai Lithium Ion.Pillar Of Physics,11 (2).

H. Perron, T Miller, C domain, J Roquest, E Simoni, R Drot, H Catalette. 2007. Structiral investigation and electronic properties of the nickel ferrite NiFe2o4:Periodic Density Functional Theory Approach; Journal Of Physics; Condens Metter 346219.

Hadiyawarman, Rijal A, Nuryadin BW. 2008. Fabrikasi Material Nanokomposit Super Kuat Dan Transparan Menggunakan Metode Simple Mixing. Jurnal Nanosains & Nanoteknologi. 2 : 1-5.

May, Gary, Light Leigh, Elshazly Dina. 1999 .Spin coating Theory. Georgia Institute of Technology.

Ismunandar. 2006. Padatan Oksida Logam Struktur, Sintesis dan Sifat sifatnya. ITB, Bandung, Hal 126. 144.

Anita, Widynugroho. 2012. Material Cerdas (2009). Blogspot. Com. Tangal akses 19 Maret 2012.

Vegunopal, Ap, Cesepedes O ; Rusell. 2014 .Controlling Dielectric and magnetic properties Of PVDF/Magnetite Nanokomposite Fiber web. International Journal Of Polymer Sains Vol 20 14, Artikel id 102946.

Siti Sofiah, Muflihatun, dan Suharyadi, Edi. 2015. Sintesis Nanopartikel Nikel Ferrite (NiFe2O4) dengan Metode Kopresifitasi dan karakterissi Sifat Kemagnetannya. Universits Gajah Mada, Yogykarta, Indo, Journal Fisika Indonesia. No. 55 vol. XIX Edisi November 2015.




DOI: http://dx.doi.org/10.24036/9846171074